ECH4404L - Separations and Mass Transfer
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 Batch Distillation



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Gas Absorption
Liquid-Liquid Extraction
Continuous Distillation
Batch Distillation
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Batch Distillation

Purpose

The goal of this laboratory exercise is to study the performance of a binary distillation column while operating in batch mode. The batch distillation column is also known as the East Column. The continuous distillation column is known as the West column.

Learning Objectives

The main learning objective of this laboratory exercise is to gain experience in fully characterizing the behavior of a binary distillation column run in batch mode. To do this, one must examine such parameters as the composition of the distillate and bottoms product, Murphree efficiency, and heat transfer properties as a function of time for the column run at various reflux rates (total and constant). These parameters should calculated theoretically using available computer programs and determined experimentally from the column.

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